Organic Structural Spectroscopy; Joseph Lambert, Scott Gronert; 2013

Organic Structural Spectroscopy Upplaga 2

av Joseph Lambert, Scott Gronert
Chapter 1 Introduction
1-1    The Spectroscopic Approach to Structure Determination
1-2    Contributions of Different Forms of Spectroscopy
1-3    The Electromagnetic Spectrum
1-4    Molecular Weight and Molecular Formula
1-5    Structural Isomers and Stereoisomers
Problems

Part I  NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY

Chapter 2 Introduction
2-1    Magnetic Properties of Nuclei
2-2    The Chemical Shift
2-3    Excitation and Relaxation
2-4    Pulsed Experiments
2-5    The Coupling Constant
2-6    Quantification and Complex Splitting
2-7    Commonly Studied Nuclides
2-8    Dynamic Effects
2-9    Spectra of Solids
2-10    Experimental Methods
Problems
Tips on Solving NMR Problems
Bibliography

Chapter 3 The Chemical Shift
3-1    Factors That Influence Proton Shifts
3-2    Proton Chemical Shifts and Structure
3-3    Medium and Isotope Effects
3-4    Factors That Influence Carbon Shirts
3-5    Carbon Chemical Shifts and Structure
3-6    Tables of Chemical Shifts
Problems
Further Tips on Solving NMR Problems
Bibliography

Chapter 4 The Coupling Constant
4-1    First-Order Spectra
4-2    Chemical and Magnetic Equivalence
4-3    Signs and Mechanisms
4-4    Couplings over One Bond
4-5    Geminal Couplings
4-6    Vicinal Couplings
4-7    Long-Range Couplings
4-8    Spectral Analysis
4-9    Second-Order Spectra
4-10    Tables of Coupling Constants
Problems
Bibliography

Chapter 5 Further Topics in One-Dimensional NMR
5-1    Spin-Lattice and Spin-Spin Relaxation
5-2    Reactions on the NMR Time Scale
5-3    Multiple Resonance
5-4    The Nuclear Overhauser Effect
5-5    Spectral Editing
5-6    Sensitivity Enhancement
5-7    Carbon Connectivity
5-8    Phase Cycling, Composite Pulses, and Shaped Pulses
Problems
Bibliography

Chapter 6 Two-Dimensional NMR
6-1    Proton-Proton Correlation Through Coupling
6-2    Proton-Heteronucleus Correlation
6-3    Proton-Proton Correlation Through Space or Chemical Exchange
6-4    Carbon-Carbon Correlation
6-5    Higher Dimensions
6-6    Pulsed Field Gradients
6-7    S...
Chapter 1 Introduction
1-1    The Spectroscopic Approach to Structure Determination
1-2    Contributions of Different Forms of Spectroscopy
1-3    The Electromagnetic Spectrum
1-4    Molecular Weight and Molecular Formula
1-5    Structural Isomers and Stereoisomers
Problems

Part I  NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY

Chapter 2 Introduction
2-1    Magnetic Properties of Nuclei
2-2    The Chemical Shift
2-3    Excitation and Relaxation
2-4    Pulsed Experiments
2-5    The Coupling Constant
2-6    Quantification and Complex Splitting
2-7    Commonly Studied Nuclides
2-8    Dynamic Effects
2-9    Spectra of Solids
2-10    Experimental Methods
Problems
Tips on Solving NMR Problems
Bibliography

Chapter 3 The Chemical Shift
3-1    Factors That Influence Proton Shifts
3-2    Proton Chemical Shifts and Structure
3-3    Medium and Isotope Effects
3-4    Factors That Influence Carbon Shirts
3-5    Carbon Chemical Shifts and Structure
3-6    Tables of Chemical Shifts
Problems
Further Tips on Solving NMR Problems
Bibliography

Chapter 4 The Coupling Constant
4-1    First-Order Spectra
4-2    Chemical and Magnetic Equivalence
4-3    Signs and Mechanisms
4-4    Couplings over One Bond
4-5    Geminal Couplings
4-6    Vicinal Couplings
4-7    Long-Range Couplings
4-8    Spectral Analysis
4-9    Second-Order Spectra
4-10    Tables of Coupling Constants
Problems
Bibliography

Chapter 5 Further Topics in One-Dimensional NMR
5-1    Spin-Lattice and Spin-Spin Relaxation
5-2    Reactions on the NMR Time Scale
5-3    Multiple Resonance
5-4    The Nuclear Overhauser Effect
5-5    Spectral Editing
5-6    Sensitivity Enhancement
5-7    Carbon Connectivity
5-8    Phase Cycling, Composite Pulses, and Shaped Pulses
Problems
Bibliography

Chapter 6 Two-Dimensional NMR
6-1    Proton-Proton Correlation Through Coupling
6-2    Proton-Heteronucleus Correlation
6-3    Proton-Proton Correlation Through Space or Chemical Exchange
6-4    Carbon-Carbon Correlation
6-5    Higher Dimensions
6-6    Pulsed Field Gradients
6-7    S...
Upplaga: 2a upplagan
Utgiven: 2013
ISBN: 9781292039565
Förlag: Pearson
Format: Häftad
Språk: Engelska
Sidor: 464 st
Chapter 1 Introduction
1-1    The Spectroscopic Approach to Structure Determination
1-2    Contributions of Different Forms of Spectroscopy
1-3    The Electromagnetic Spectrum
1-4    Molecular Weight and Molecular Formula
1-5    Structural Isomers and Stereoisomers
Problems

Part I  NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY

Chapter 2 Introduction
2-1    Magnetic Properties of Nuclei
2-2    The Chemical Shift
2-3    Excitation and Relaxation
2-4    Pulsed Experiments
2-5    The Coupling Constant
2-6    Quantification and Complex Splitting
2-7    Commonly Studied Nuclides
2-8    Dynamic Effects
2-9    Spectra of Solids
2-10    Experimental Methods
Problems
Tips on Solving NMR Problems
Bibliography

Chapter 3 The Chemical Shift
3-1    Factors That Influence Proton Shifts
3-2    Proton Chemical Shifts and Structure
3-3    Medium and Isotope Effects
3-4    Factors That Influence Carbon Shirts
3-5    Carbon Chemical Shifts and Structure
3-6    Tables of Chemical Shifts
Problems
Further Tips on Solving NMR Problems
Bibliography

Chapter 4 The Coupling Constant
4-1    First-Order Spectra
4-2    Chemical and Magnetic Equivalence
4-3    Signs and Mechanisms
4-4    Couplings over One Bond
4-5    Geminal Couplings
4-6    Vicinal Couplings
4-7    Long-Range Couplings
4-8    Spectral Analysis
4-9    Second-Order Spectra
4-10    Tables of Coupling Constants
Problems
Bibliography

Chapter 5 Further Topics in One-Dimensional NMR
5-1    Spin-Lattice and Spin-Spin Relaxation
5-2    Reactions on the NMR Time Scale
5-3    Multiple Resonance
5-4    The Nuclear Overhauser Effect
5-5    Spectral Editing
5-6    Sensitivity Enhancement
5-7    Carbon Connectivity
5-8    Phase Cycling, Composite Pulses, and Shaped Pulses
Problems
Bibliography

Chapter 6 Two-Dimensional NMR
6-1    Proton-Proton Correlation Through Coupling
6-2    Proton-Heteronucleus Correlation
6-3    Proton-Proton Correlation Through Space or Chemical Exchange
6-4    Carbon-Carbon Correlation
6-5    Higher Dimensions
6-6    Pulsed Field Gradients
6-7    S...
Chapter 1 Introduction
1-1    The Spectroscopic Approach to Structure Determination
1-2    Contributions of Different Forms of Spectroscopy
1-3    The Electromagnetic Spectrum
1-4    Molecular Weight and Molecular Formula
1-5    Structural Isomers and Stereoisomers
Problems

Part I  NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY

Chapter 2 Introduction
2-1    Magnetic Properties of Nuclei
2-2    The Chemical Shift
2-3    Excitation and Relaxation
2-4    Pulsed Experiments
2-5    The Coupling Constant
2-6    Quantification and Complex Splitting
2-7    Commonly Studied Nuclides
2-8    Dynamic Effects
2-9    Spectra of Solids
2-10    Experimental Methods
Problems
Tips on Solving NMR Problems
Bibliography

Chapter 3 The Chemical Shift
3-1    Factors That Influence Proton Shifts
3-2    Proton Chemical Shifts and Structure
3-3    Medium and Isotope Effects
3-4    Factors That Influence Carbon Shirts
3-5    Carbon Chemical Shifts and Structure
3-6    Tables of Chemical Shifts
Problems
Further Tips on Solving NMR Problems
Bibliography

Chapter 4 The Coupling Constant
4-1    First-Order Spectra
4-2    Chemical and Magnetic Equivalence
4-3    Signs and Mechanisms
4-4    Couplings over One Bond
4-5    Geminal Couplings
4-6    Vicinal Couplings
4-7    Long-Range Couplings
4-8    Spectral Analysis
4-9    Second-Order Spectra
4-10    Tables of Coupling Constants
Problems
Bibliography

Chapter 5 Further Topics in One-Dimensional NMR
5-1    Spin-Lattice and Spin-Spin Relaxation
5-2    Reactions on the NMR Time Scale
5-3    Multiple Resonance
5-4    The Nuclear Overhauser Effect
5-5    Spectral Editing
5-6    Sensitivity Enhancement
5-7    Carbon Connectivity
5-8    Phase Cycling, Composite Pulses, and Shaped Pulses
Problems
Bibliography

Chapter 6 Two-Dimensional NMR
6-1    Proton-Proton Correlation Through Coupling
6-2    Proton-Heteronucleus Correlation
6-3    Proton-Proton Correlation Through Space or Chemical Exchange
6-4    Carbon-Carbon Correlation
6-5    Higher Dimensions
6-6    Pulsed Field Gradients
6-7    S...
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Om Organic Structural Spectroscopy (2013)

I november 2013 släpptes boken Organic Structural Spectroscopy skriven av Joseph Lambert, Scott Gronert. Det är den 2a upplagan av kursboken. Den är skriven på engelska och består av 464 sidor djupgående information. Förlaget bakom boken är Pearson som har sitt säte i London.

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